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CAS: 92-39-7
分子式: C12H8ClNS
分子量: 233.72
熔点: 197-202℃
中文名称: 
2-氯吩噻嗪
2-氯-10H-吩噻嗪
英文名称: 
10H-Phenothiazine,2-chloro-
2-Chlorophenothiazine
2-chloro-10H-Phenothiazine
2-chloro-phenothiazin
2-chloro-10h-phenothiazin
2-chlorophenthiazine
2-Chlorothiodiphenylamine
性质描述: 熔点196-199℃(分解)。
生产方法: 由间氯二苯胺经环合而得。在反应锅内加入间氯二苯胺和硫磺,升温至70℃,加入碘。升温至120℃,减压排出硫化氢,再升温至168-172℃,保温0.5h。冷却,加入氯苯和活性炭,加热回流1h。趁热过滤,滤液冷至15℃结晶。甩滤,用氯苯、乙醇洗涤滤饼各1次,得2-氯吩噻嗪。
用途: 医药中间体,用于制备氯丙嗪、奋乃静。
推荐供应商
货号品牌产品名称规格包装、参考价格详情
C804527MACKLIN2-氯吩噻嗪98%58元/25g;   163元/100g;   展开
储存:2~8°C
状态:黄色到灰色到绿色到棕色粉末
C0248TCI2-Chlorophenothiazine>98.0%(GC)245元/25G;   1890元/500G;   展开

基本信息

纯度/分析方法>98.0%(GC)
分子式/分子量C12H8ClNS = 233.71
外观与形状(20℃)固体
Reaxys-RN176587
PubChem物质ID87565408
SDBS (AIST Spectral DB)7022
MDL编号MFCD00005016

技术规格

AppearanceWhite to Light yellow to Green powder to crystal
Purity(GC)min. 98.0 %
Melting point198.0 to 203.0 ℃

物性(参考值)

熔点198 ℃
水溶性微溶
溶解性(可溶于)乙醇,丙酮,苯,乙醚

安全信息

图形或危害标志
信号词警告
危险性说明H315 : 造成皮肤刺激。
H319 : 造成严重眼刺激。
防范说明P264 : 作业后彻底清洗皮肤。
P280 : 戴防护手套/戴防护眼罩/戴防护面具。
P302 + P352 : 如皮肤沾染:用水充分清洗。
P337 + P313 : 如仍觉眼刺激:求医/就诊。
P305 + P351 + P338 : 如进入眼睛:用水小心冲洗几分钟。如戴隐形眼镜并可方便地取出,取出隐形眼镜。继续冲洗。
P362+P364 : 脱掉沾污的衣服,清洗后方可重新使用。
P332 + P313 : 如发生皮肤刺激:求医/就诊。

相关法规

RTECS#SN7580000
378253J&K2-Chlorophenothiazine98%234元/25G;   785元/100G;   2001元/500G;   展开

基本信息

分子式C12H8ClNS
分子量233.72
熔点195-200
MDL编码MFCD00005016
Beilstein176587
EINECS 编号202-152-5

安全信息

图形或危害标志
提示语Warning
危险说明H315
H319
H335
防范说明P261
P305+P351+P338
WGK3
RTECSSN7580000
Y0000508Chlorpromazine impurity EEuropean Pharmacopoeia (EP) Reference Standard1277.32元/ ;   展开

产品说明

一般描述

This product is provided as delivered and specified by the issuing Pharmacopoeia. All information provided in support of this product, including SDS and any product information leaflets have been developed and issued under the Authority of the Issuing Pharmacopoeia. For further information and support please go to the website of the issuing Pharmacopoeia.

包装

Unit quantity: 10 mg. Subject to change. The product is delivered as supplied by the issuing Pharmacopoeia. For the current unit quantity, please visit the EDQM reference substance catalogue.

注意

Please find SDS provided by EDQM here..

其他说明

Sales restrictions may apply.

基本信息

经验(实验)分子式C12H8ClNS
分子量233.72
Beilstein176587
MDL编号MFCD00005016
PubChem化学物质编号329830991
NACRESNA.24

产品性质

等级pharmaceutical primary standard
manufacturer/tradenameEDQM
mp195-200 ℃ (lit.)
application(s)pharmaceutical (small molecule)
格式neat
储存温度2-8℃
SMILES stringClc1ccc2Sc3ccccc3Nc2c1
InChI1S/C12H8ClNS/c13-8-5-6-12-10(7-8)14-9-3-1-2-4-11(9)15-12/h1-7,14H
InChI keyKFZGLJSYQXZIGP-UHFFFAOYSA-N

安全信息

象形图GHS07
警示用语:Warning
危险声明H317
预防措施声明P261 - P272 - P280 - P302 + P352 - P333 + P313 - P362 + P364
危险分类Skin Sens. 1
储存分类代码11 - Combustible Solids
WGKWGK 3
闪点(F)Not applicable
闪点(C)Not applicable
C63006Sigma-Aldrich2-Chlorophenothiazine97%425.87元/25 G;   展开

基本信息

经验(实验)分子式C12H8ClNS
分子量233.72
Beilstein176587
EC 号202-152-5
MDL编号MFCD00005016
PubChem化学物质编号24892856
NACRESNA.22

产品性质

测定97%
mp195-200 ℃ (lit.)
SMILES stringClc1ccc2Sc3ccccc3Nc2c1
InChI1S/C12H8ClNS/c13-8-5-6-12-10(7-8)14-9-3-1-2-4-11(9)15-12/h1-7,14H
InChI keyKFZGLJSYQXZIGP-UHFFFAOYSA-N

安全信息

象形图GHS07
警示用语:Warning
危险声明H317
预防措施声明P261 - P272 - P280 - P302 + P352 - P333 + P313 - P362 + P364
危险分类Skin Sens. 1
储存分类代码11 - Combustible Solids
WGKWGK 3
闪点(F)Not applicable
闪点(C)Not applicable
个人防护装备dust mask type N95 (US), Eyeshields, Gloves
216561Fluorochem2-Chloro-10H-phenothiazine95%220元/1g;   286元/25g;   836元/100g;   展开

基本信息

CAS Number92-39-7
MDL NumberMFCD00005016
Melting Point198℃

安全信息

图形或危害标志
危险性说明 H315: Causes skin irritation.
H319: Causes serious eye irritation.
H335: May cause respiratory irritation.
防范说明 P233: Keep container tightly closed.
P260: Do not breathe .
P261: Avoid breathing .
P264: Wash hands thoroughly after handling.
P271: Use only outdoors or in a well-ventilated area.
P280: Wear .
P302 + P352: IF ON SKIN: Wash with plenty of soap and water.
P304: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing..
P304 + P340: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P312: Call a POISON CENTER or doctor/physician if you feel unwell.
P321: Specific treatment (see relevant procedures. on this label).
P332 + P313: If skin irritation occurs: Get medical advice/ attention.
P337 + P313: If eye irritation persists: Get medical advice/attention.
P340: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P362: Take off contaminated clothing and wash before reuse.
P403: Store in a well-ventilated place.
P403 + P233: Store in a well-ventilated place. Keep container tightly closed.
P405: Store locked up.
P501: Dispose of contents/container to in accordance with local regulation .
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