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CAS: 108-13-4
分子式: C3H6N2O2
分子量: 102.09
熔点: 166-172℃
中文名称: 
丙二酰胺
英文名称: 
Propanediamide
malonamide
carboxamidoacetamide
malondiamide
malonic acid diamide
malonic diamide
malonyldiamide
Malonamid
性质描述: 白色单斜针状结晶。熔点170℃(171.5-172.5℃)。在8℃水中的溶解度为8.3g/100ml,不溶于醇、醚和苯。
生产方法: 由丙二酸二乙酯与氨反应而得。将氨水加入搪瓷桶内,冷至25℃以下,在搅拌下慢慢加入丙二酸二乙酯,反应温度在20℃左右,反应完后在室温放置两天。滤出底部结晶,减压浓缩,加入脱色炭,经抽滤,冷却结晶,于80℃干燥,粉碎即为成品。
用途: 用于有机合成。
推荐供应商
货号品牌产品名称规格包装、参考价格详情
M813085MACKLIN丙二酰胺98%30元/5g;   102元/25g;   364元/100g;   1589元/500g;   6850元/2.5kg;   展开
储存:室温, 密封
状态:白色至类白色粉末或固体或块状物
M0027TCIMalonamide>98.0%(N)190元/25G;   550元/100G;   1890元/500G;   展开

基本信息

纯度/分析方法>98.0%(N)
分子式/分子量C3H6N2O2 = 102.09
外观与形状(20℃)固体
Reaxys-RN1751401
PubChem物质ID87572145
SDBS (AIST Spectral DB)3629
MDL编号MFCD00008034

技术规格

AppearanceWhite to Almost white powder to crystal
Purity(with Total Nitrogen)min. 98.0 %
Melting point169.0 to 175.0 ℃

物性(参考值)

熔点174 ℃

相关法规

RTECS#ON9125000
515770J&KMalonamide98%223元/25G;   733元/100G;   3366元/500G;   展开

基本信息

分子式C3H6N2O2
分子量102.09
熔点172-175
MDL编码MFCD00008034
Beilstein1751401
EINECS 编号203-553-8

安全信息

WGK2
RTECSON9125000
A17939Alfa AesarMalonamide98%1713元/100g;   6837元/500g;   25554元/2500g;   展开

应用
Malonamide is a reagent for fluorimetric determination of reducing carbohydrates. The malonamide-based ionic liquid extractant was used in the extraction of europium(iii) and other trivalent rare earth elements from nitric acid medium.

备注
Store in cool, dry place in a well sealed container. Store away from oxidizing agents.

基本信息

MDL
MFCD00008034

EINECS
203-553-8

分子式
C3H6N2O2

分子量
102.09

熔点
167-171°

灵敏度
Ambient temperatures.

形态
Powder

溶解性
Soluble in HCl.

Beilstein
1751401

安全信息

RTECS
ON9125000

TSCA

129593Sigma-AldrichMalonamide97%802.37元/100 G;   展开

产品说明

一般描述

丙二酰胺衍生物是通过异氰酸酯、Meldrum′s酸、芳叉丙二腈和CH 2 Cl 2 中两个胺分子的一锅五组分缩合反应产生的。

应用

离子液体萃取剂用于从硝酸介质中萃取铕(iii)等三价稀土离子 。

包装

100 g in poly bottle

基本信息

线性分子式CH2(CONH2)2
分子量102.09
Beilstein1751401
EC 号203-553-8
MDL编号MFCD00008034
PubChem化学物质编号24847915
NACRESNA.22

产品性质

质量水平100
测定97%
mp172-175 ℃ (lit.)
荧光λex 367 nm; λem 445 nm (α-keto acid adduct)
SMILES stringNC(=O)CC(N)=O
InChI1S/C3H6N2O2/c4-2(6)1-3(5)7/h1H2,(H2,4,6)(H2,5,7)
InChI keyWRIRWRKPLXCTFD-UHFFFAOYSA-N

安全信息

储存分类代码13 - Non Combustible Solids
WGKWGK 2
闪点(F)Not applicable
闪点(C)Not applicable
个人防护装备Eyeshields, Gloves, type N95 (US)
094932FluorochemMalonamide97%264元/25g;   924元/100g;   4312元/500g;   展开

基本信息

CAS Number108-13-4
MDL NumberMFCD00008034
Melting Point174℃

安全信息

图形或危害标志
危险性说明 H315: Causes skin irritation.
H319: Causes serious eye irritation.
H335: May cause respiratory irritation.
防范说明 P233: Keep container tightly closed.
P260: Do not breathe .
P261: Avoid breathing .
P264: Wash hands thoroughly after handling.
P271: Use only outdoors or in a well-ventilated area.
P280: Wear .
P302 + P352: IF ON SKIN: Wash with plenty of soap and water.
P304: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing..
P304 + P340: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P312: Call a POISON CENTER or doctor/physician if you feel unwell.
P321: Specific treatment (see relevant procedures. on this label).
P332 + P313: If skin irritation occurs: Get medical advice/ attention.
P337 + P313: If eye irritation persists: Get medical advice/attention.
P340: Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P362: Take off contaminated clothing and wash before reuse.
P403: Store in a well-ventilated place.
P403 + P233: Store in a well-ventilated place. Keep container tightly closed.
P405: Store locked up.
P501: Dispose of contents/container to in accordance with local regulation .
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